600 MHz Nuclear Magnetic Resonance Spectrometer (Magic)
Slovenian NMR Centre in Ljubljana
Nuclear Magnetic Resonance spectroscopy is a research technique that exploits atomic nuclei with non-zero magnetic moments to act as tiny probes for the detection of the local structure, dynamics, reaction state and chemical environment within molecules. NMR spectra are unique, well-resolved, analytically tractable and often highly predictable for small molecules. NMR analysis is therefore used for confirming the identity of a substance. Different functional groups are easily distinguishable and identical functional groups with differing neighbors still give distinguishable signals. NMR is also a valuable tool for studying local structure and dynamics in a variety of solid systems. Objects of such solid-state NMR studies in materials science are inorganic/organic aggregates in crystalline and amorphous states, composite materials, heterogeneous systems including liquid or gas components, suspensions and molecular aggregates with dimensions on the nanoscale.
Technical specifications Agilent Technologies VNMRS 600 MHz
| Magnet: | 14.1 Tesla 51 mm bore Oxford Superconducting Magnet |
| System: | Red Hat 6.1 |
| Software: | VNMRJ rev. 3.2A |
| Probe 1: | 5mm 1H{13C/15N} PFG Triple Probe (from -20oC to +80oC) |
| Probe 2: | 5mm 1H{13C/15N/31P} PFG Penta Probe (from -100oC to +120oC) |
| Probe 3: | 5mm 13C-31P Broadband Probe (from -150oC to +200oC) |
| Probe 4: | 5mm low-gamma Broadband Probe (from -80oC to +130oC) |
| Probe 5: | 5mm 1H{15N-31P} PFG Indirect Probe (from -50oC to +50oC) |
| Probe 6: | 4mm 1H Nano Probe (from -150oC to +200oC) |
| Probe 7: | 3.2mm Double Resonance HX MAS Probe (Varian) (from -40oC to +100oC) |
| Probe 8: | 1.6mm Triple Resonance HXY FastMAS Probe (Varian) (from 0oC to +70oC) |
| Probe 9: | 5mm Triple Resonance HXY SupersonicMAS Probe (Doty) (from -40oC to +70oC) |
| Probe 10: | 4 mm Double Resonance HX HotMAS (Custom made) (from +30oC to +320oC) |
Sample environment
Detailed information can be found on the Instrument’s webpage.
Contact:
Janez Plavec (tel:+386 147 60 353)
Maja Marušic (tel: +386 318 42 113)